EDIT: I did the titration. I applied 500ml of my stock solution HCl, and titrated from my stock solution of NaOH. HCl is 0.001M and NaOH is 5M. When likely this route, a simple polar wash (like a sodium carbonate clean) with your nonpolar solvent is practically a must; without having it, the products is typically harsher to smoke. four. Faste